Chemical Engineering Lab Equipment's

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In an ideal Plug Flow Reactor (PFTR) there is no mixing in the direction of flow and complete mixing perpendicular to direction of flow. Concentration of reactants varies along the length of reactor but not in radial direction. This set-up is used to study a non-catalytic homogeneous reaction under ambient condition. The set up consists of two feed tanks through which two reactants are fed to the reactor. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The compressed air is used for circulation of feed. Samples are collected for analysis from the outlet of reactor. Pressure Regulator, Pressure Gauge and Safety Valve are fitted in the compressed air line.

Experimentation:

• Sponification Reaction Study in straight tube Plug Flow Reactor.
• To determine Reaction Rate Constant.

• Feed Tank (2Nos.): Material Stainless Steel, Capacity - 20 Ltrs.
• Feed Circulation: By compressed air.
• Flow Measurement: Rotameter 2 Nos. (one each for Reactants).
• Piping: Stainless Steel and PVC
• Pressure Gauge: Bourdon type 0-2 Kg/cm2.
• Stop Watch: Electronic.
• Instruction Manual: An ENGLISH instruction manual will be provided along with the Apparatus
• The whole unit is assembled rigidly on a base plate and mounted on a stand.
• Most of the parts are powder coated and rest are painted with auto paints.

• Compressed Air Supply at 2 Bar, 0.5 CFM.
• Water Supply.
• Drain.
• Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted.

Additional Information:

• Item Code: SCRE-04
• Pay Mode Terms: L/C (Letter of Credit),T/T (Bank Transfer),D/P,D/A,Other
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: wooden boxes are used if required.

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In an ideal CSTR (i.e. an ideal steady state flow reactor) the contents in reactor are well mixed and have uniform composition throughout. Thus the exit stream has the same composition as the fluid within the reactor. This type of reactor is known as mixed flow reactor. This set-up is used to study a non-catalytic homogeneous second order liquid phase reaction under isothermal condition. The set up consists of two feed tanks through which two reactants are fed to the reactor. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The compressed air is used for circulation of feed. The CSTR is fitted with stirrer for proper mixing. From top outlet of it samples are collected for analysis. Constant temperature water bath arrangement is provided to conduct the experiment at various temperatures. Pressure Regulator, Pressure Gauge and Safety Valve are fitted in the compressed air line.

Experimentation:

• Sponification Reaction study in Isothermal CSTR.
• To determine the Reaction Rate Constant and effect of temperature on it.

• Reactor: Material Stainless Steel, Capacity 2 Ltrs (Approx).
• Stirrer: Stainless Steel Impeller and shaft coupled with FHP Motor
• Feed Tank (2Nos.): Material Stainless Steel, Capacity - 20 Ltrs
• Feed Circulation: By compressed air.
• Flow Measurement: Rotameter 2Nos. (one each for Reactants).
• Piping: Stainless Steel and PVC.
• Pressure Gauge: Bourdon type 0-2 Kg/cm2
• Stop Watch: Electronic
• Control Panel comprises of: Standard make on off switch, Mains Indicator etc.
• Instruction Manual: An ENGLISH instruction manual will be provided along with the Apparatus
• The whole unit is assembled rigidly on a base plate and mounted on a stand
• Most of the parts are powder coated and rest are painted with auto paints.

• Water Supply.
• Drain.
• Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted.

Additional Information:

• Item Code: SCRE-01
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: wooden boxes are used.

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• Maintains temperature throughout
• Stainless steel used
• Optimum performance

• Sponification Reaction Study In A Combined Reactor
• Sponification Reaction Study In Coil Tube Type Plug Flow Reactor
• Sponification Reaction Study In A Mfr
• To Determine Reaction Rate Constant

• Compressed Air Supply At 2 Bar, 0.5 Cfm
• Water Supply & Drain
• Instruments, Laboratory Glassware And Chemicals Required For Analysis As Per The System Adopted

• 1st Reactor: Material Stainless Steel, Capacity 0.7 Ltrs. (Approx)
• 2nd Reactor: Material Stainless Steel, Capacity 2 Ltrs (Approx)
• Stirrer For Mfr: Stainless Steel Impeller And Shaft Coupled With Fhp Motor Remi/Eltek Make
• Feed Tank (2nos.): Material Stainless Steel, Capacity - 20 Ltrs
• Feed Circulation: By Compressed Air
• Flow Measurement: Rotameter 2 Nos. (One Each For Reactants) Eureka/Iepl Make
• Piping : Stainless Steel And Pvc
• Pressure Regulator: 0-2 Kg/Cm2 Janetics/Shavo Norgen Make
• Pressure Gauge: Bourdon Type 0-2 Kg/Cm2 Mass/Pricol Make
• Stop Watch: Electronic
• Instruction Manual: An English Instruction Manual Will Be Provided Along With The Apparatus

Additional Information:

• Item Code: SCRE-11
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: wooden boxes are used.

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• To Plot Rtd Curve For A Cstr. Using Pulse Tracer
• To Determine The Dispersion No
• Utilities Required
• Compressed Air Supply At 2 Bar, 0.25 Cfm
• Water Supply
• Drain
• Instruments, Laboratory Glassware And Chemicals Required For Analysis As Per The System Adopted

• Reactor: Material Stainless Steel, Capacity 2 Ltrs. (Approx.)
• Stirrer: Material Stainless Steel Impeller And Shaft Coupled With Fhp Motor
• Feed Tank: Material Stainless Steel, Capacity - 20 Ltrs
• Feed Circulation: By Compressed Air
• Flow Measurement: Rota Meter
• Piping: Stainless Steel And Pvc
• Pressure Gauge: Bourdon Type 0-2 Kg/Cm2
• Stop Watch: Electronic Control Panel Comprises Of : With Standard Make On/Off Switch, Mains Indicator Etc
• Instruction Manual : An English Instruction Manual Will Be Provided Along With The Apparatus
• The Whole Unit Is Assembled Rigidly On A Base Plate And Mounted On A Stand.
• Most Of The Parts Are Powder Coated And Rest Are Painted With Auto Paints.

Additional Information:

• Item Code: SCRE-14
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: wooden boxes are used.

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• To Determine Hydrodynamics Of A Trickle Bed Reactor Involving The Measurement Of Pressure Drop, Hold-Up & Flow Regime
• Utilities Required
• Compressed Air At 4 Bar
• Water Supply And Drain.

• Packed Bed: Material Borosilicate Glass Dia. 80mm, Height 600mm
• Packings: Glass Beads Dia. 3mm/Rasching Rings, Size 8-10mm
• Flow Measurement: Rotameter One Each For Water And Air
• Liquid Feed Tank: Material Stainless Steel Capacity 60 Ltrs
• Feed Circulation: Centrifugal Pump Capacity ¼ Hp Crompton/Sharpmake
• Air Tank: Compatible Capacity
• Pressure Regulator (2 Nos.): 1. Operating Range 0-2 Kg/Cm2 And O-10 Kg/Cm2
• Pressure Gauge: Bourdon Type
• Mixing Chamber: Material Stainless Steel Of Compatible Capacity For Air & Water
• Liquid Catch Pot: Material Stainless Steel Of Compatible Capacity.
• Solenoid Valve: 2 Nos. (One Each At Liquid And Air Inlet)
• Manometers: Compatible Capacity
• Piping: Material Stainless Steel And Pvc. ½” Line Size
• Control Valves: Material Gun Metal/Brass
• Control Panel Comprising Of Standard Make On Off Switch, Mains Indicator Etc
• Instruction Manual: An English Instruction Manual Will Be Provided Along With The Apparatus A Good Quality Painted Rigid Ms Structure Is Provided To Support All The Parts

Additional Information:

• Item Code: SCRE-17
• Pay Mode Terms: L/C (Letter of Credit),T/T (Bank Transfer),D/P,D/A,Other
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: WOODEN BOXES IF REQUIRED.

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Batch reactor is a closed system with no input and output streams. A batch reactor can operate under conditions like isothermal (temperature of reaction mass remains constant), perfectly mixed (composition of reaction mixture is uniform throughout), and constant volume (volume of the reaction mixture within the reactor remains constant, there is no appreciable change in the density of reaction mass). This set-up is used to study a non-catalytic homogeneous reaction under isothermal condition. The set up consists of a reactor fitted in a constant temperature water bath. One stirrer is fitted for mixing the reactants in reactor and other is fitted in water bath to keep the uniform temperature throughout in the bath. The temperature of bath can be maintained from ambient to 90c with the help of digital temperature indicator cum controller. Samples can be taken out with the help of a sampling pipette.

Experimentation:

• to study the progress of a chemicals reaction and determine the kinetic parameters.
• to determine the effect of temperature on reaction rate constant.

• Water Supply.
• Drain.
• Instruments, laboratory glassware and chemicals required for analysis as per the system adopted.

• Reactor: material stainless steel, volume- 1 ltrs. (approx. )
• Water bath: material stainless steel, double wall, insulated with ceramic wool.
• Heater: nichrome wire heater
• Stirrer (2 nos. ): stainless steel impeller and shaft coupled with fhp motor.
• Stop watch: electronic
• Temp. Sensor: rtd pt-100 type
• Control panel comprises of: digital temp.
• Controller: 0-199. 9°c, rtdø pt-100 type(for water bath) cum-indicator with standard make on/off switch, mains indicator fuse etc.
• instruction manual: an english instruction manual will be provided along with the apparatus. the whole unit is assembled rigidly on a base plate and mounted on a stand.

Additional Information:

• Item Code: SCRE-07
• Pay Mode Terms: L/C (Letter of Credit),T/T (Bank Transfer),D/P,D/A,Other
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: WOODEN BOXES IF REQUIRED.

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• To Determine The Reaction Rate Constant
• Utilities Required
• Water Supply
• Drain.
• Instruments, Laboratory Glassware And Chemicals Required For Analysis As Per The System Adopted

• Packing: Catalyst (Fluid Bed Type)
• Feed Tank (1nos.): Material Stainless Steel, Capacity - 20 Ltrs
• Flow Measurement: Rota Meter 2nos.(One Each For Feed & Recycled Product)
• Piping: Stainless Steel And Pvc. Size ¼”
• Feed Circulation: Magnetic Pump Of Poly Propylene
• Hot Water Tank: Made Of Stainless Steel, Double Wall, Insulated With Ceramic Wool Capacity: 10-15 Ltrs
• Hot Water Circulation: Magnetic Pump Of Poly Propylene To Circulate Hot
• (In Outer Jacket) Water Maximum Working Temp. 850 C
• Control Panel Comprises Of: Digital Temp. Controller: 0-199.9°C (For Hot Water Bath) With Standard Make On/Off Switch, Mains Indicator Etc
• Instruction Manual: An English Instruction Manual Will Be Provided Along With The Apparatus
• The Whole Unit Is Assembled Rigidly On A Base Plate And Mounted On A Stand.
• Most Of The Parts Are Powder Coated And Rest Are Painted With Auto Paints.

Additional Information:

• Item Code: SCRE-21
• Pay Mode Terms: L/C (Letter of Credit),T/T (Bank Transfer),D/P,D/A,Other
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: WOODEN BOXES IF REQUIRED.

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• Sponification Reaction study in Isothermal CSTR.
• To determine the Reaction Rate Constant and effect of temperature on it

• Reactor: Material Stainless Steel, Capacity 2 Ltrs. (Approx).
• Water Bath: Material Stainless Steel, Double wall, insulated with Ceramic Wool
• Heater: Nichrome wire Heater
• Stirrer (2Nos.): Stainless Steel Impeller and shaft coupled with FHP motor. (One each for Water Bath and Reactor).
• Feed Tank (2Nos.): Material Stainless Steel, Capacity - 20 Ltrs.
• Feed Circulation: By compressed air.
• Flow Measurement: Rotameter 2 Nos. one each for Reactants.
• Piping: Stainless Steel and PVC.
• Pressure Regulator: 0-2 Kg/cm2
• Pressure Gauge: Bourdon type 0-2 Kg/cm2
• Stop Watch: Electronic
• Temp. Sensor: RTD PT-100 type
• Control panel comprises of : Digital Temp. Controller : 0-199.9°C (For Hot Water Bath) With Standard make on/off switch, Mains Indicator etc.
• Instruction Manual: An ENGLISH instruction manual will be provided along with the Apparatus The whole unit is assembled rigidly on a base plate and mounted on a stand.

• Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted.

Additional Information:

• Item Code: SCRE-02
• Pay Mode Terms: L/C (Letter of Credit),T/T (Bank Transfer),D/P,D/A,Other
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: WOODEN BOX IF REQUIRED.

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The unit designed to perform the saccharose hydrolysis reaction in a continuous way by using catalytic fixed-bed reactors. Saccharose hydrolysis is the industrial process to obtain glucose and frustose from saccharose. It is a reversible chemical reaction.

Experimentation:

• Study of the principles of catalytic fixed-bed reactors.
• Effect of the variation in the particle´s size in the effectiveness of a fixed-bed reactor.
• Comparison of chemical and biological (enzymic) catalysis.
• Checking the influence on different variables (feed flow, temperature of reaction, reagents concentration) on the obtained final product
• Effect of flow rate, temperature and feed concentration on steady state conversion
• Tracer studies to characterize fluid flow within the reactors

• Bench-top unit. and panels in painted steel.
• Main metallic elements in stainless steel.
• Diagram in the front panel with similar distribution to the elements in the real unit.
• 2 Glass flacks of 2 litres of capacity, for the initial solution and the final product.
• Reactors: Two fixed-bed reactors for chemical catalysis, composed by acid ion exchange resins.
• A fixed-bed reactor for biological (enzymic) catalysis. (Recommended use with an immobilized enzyme).
• Reactors diameter: 50 mm. Reactors height: 160 mm. Material: glass, with a methacrylate cover for protection.
• Thermostatic bath, with heating resistance of 600W.
• A heated water supply to the reactors jackets allows the automatic control of reaction temperature to a set point value.
• Peristaltic pump, with speed regulation, that allows to regulate the feed flow from 0 to 32 ml/min.
• 4 Temperature sensors, “J“ type, placed at key points of the system.
• All electrical circuits are protected by adequate protection devices.
• Electronic console: Metallic box. Connections for the temperature sensors. Digital display for the temperature sensors. Selector for the temperature sensors. Heating resistance controller. Digital display for feeding flow.
• Pump switch. Pump regulator (potentiometer). Cables and Accessories, for normal operation.
• Manuals: This unit is supplied with the following manuals: Required Services, Assembly and Installation, Starting-up, Safety, Maintenance & Practices Manuals.

Additional Information:

• Item Code: SCRE-24
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: Wooden boxes are used.

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DESCRIPTION: In an ideal Plug Flow Reactor (PFTR) there is no mixing in the direction of flow and complete mixing perpendicular to direction of flow. Concentration of reactants varies along the length of reactor but not in radial direction. In case of a coil turbulence is introduced due to frequent change in direction of flow and presence of secondary flow, so a higher value of reaction rate constant is expected in coil tube type plug flow reactor. This set-up is used to study a non-catalytic homogeneous reaction under isothermal condition. The set up consists of two feed tanks through which two reactants are fed to the reactor. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The compressed air is used for circulation of feed. It is a helical coil tube type reactor kept in a constant temperature water bath to conduct the experiment at various temperatures. Reactants enter at lower end coming out of the top of coil from where samples are collected for analysis. Pressure Regulator, Pressure Gauge and Safety Valve are fitted in the compressed air line.

EXPERIMENTATION:

Ø Sponification Reaction study in Isothermal Plug Flow Reactor.

Ø To determine Reaction Rate Constant and effect of temperature on it.

TECHNICAL DETAILS :

Ø Reactor : Material Stainless Steel, Capacity 0.7 Ltrs. (approx) (Helical Coiled Tube Type)

Ø Water Bath : Material Stainless Steel, Double wall, insulated with CeramicWool.

Ø Heater : Nichrome wire Heater

Ø Stirrer (Water Bath) : Material SS Impeller and shaft coupled with FHP motor

Ø Feed Tank (2Nos.) : Capacity - 20 Ltrs.

Ø Feed Circulation : By compressed air.

Ø Flow Measurement : Rotameter 2Nos. one each for Reactants

Ø Piping : Stainless Steel and PVC.

Ø Pressure Regulator : 0-2 K

Ø Control panel comprises of Standard make on/off switch, Mains Indicator etc.

Ø Digital Temp. Controller : 0-200°C, RTD PT-100 type (For Water Bath)

Ø Instruction Manual : An ENGLISH instruction manual will be provided along with the Apparatus

Ø The whole unit is assembled rigidly on a base plate and mounted on a stand.

Ø Most of the parts are powder coated and rest are painted with auto paints.

Additional Information:

• Item Code: SCRE-06
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: Wooden boxes are used.

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A isothermal semi-batch reactor is a semi-closed system with one input stream. It is operated under conditions like isothermal (temperature of reaction mass remains constant) and perfectly mixed (composition of reaction mixture is uniform throughout). This set-up is used to study a non-catalytic homogeneous reaction under isothermal condition.

the set up consists of a reactor fitted in a constant temperature water bath. Before starting the reaction the reactor is charged with measured quantity of one reactant. From a feed tank another reactant is fed to the reactor. Using a sampling pipette samples can be taken out for analysis after fixed interval. Rotameter is provided to measure the flow of chemicals. The compressed air is used for circulation of feed. One stirrer is fitted for mixing the reactants in reactor and other is fitted in water bath to keep the uniform temperature throughout in the bath. The temperature of bath can be maintained from ambient to 70c with the help of digital temperature indicator cum controller. Pressure regulator, pressure gauge and safety valve are fitted in the compressed air line.

Experimentation:

• To study a second order sponification reaction in a semi-batch reactor.
• To determine the reaction rate constant.

• Reactor: Material Stainless Steel, Capacity 3 Ltrs. (Approx).
• Water Bath: Material Stainless Steel, Double Wall, Insulated With Ceramic Wool.
• Heater: Nichrome Wire Heater
• Stirrer: Material Stainless Steel Impeller And Shaft Coupled With Fhp Motor
• Feed Tank (1Nos. ): Material Stainless Steel, Capacity - 20 Ltrs.
• Feed Circulation: By Compressed Air.
• Flow Measurement: Rotameter.
• Piping: Material Stainless Steel And Pvc.
• Stop Watch: Electronic
• Temp. Sensor: Rtd Pt-100 Type
• Control Panel Comprises Of: Digital Temp.
• Controller: 0-199. 9°C, Rtd Pt-100 Type (For Water Bath) With Standard Make On/Off Switch, Mains Indicator Etc.
• Instruction Manual: An English Instruction Manual Will Be Provided Along With The Apparatus
• The Whole Unit Is Assembled Rigidly On A Base Plate And Mounted On A Stand.
• Most Of The Parts Are Powder Coated And Rest Are Painted With Auto Paints.

Additional Information:

• Item Code: SCRE-08
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: WOODEN BOXES IF REQUIRED.

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DESCRIPTION :                                                                                 An adiabatic batch reactor is a closed system with no input and output streams. This reactor is operated under conditions like adiabatic (Temperature of Reaction Mass keep on changing), perfectly mixed (composition of reaction mixture is uniform throughout), and constant volume (volume of the reaction mixture within the reactor remains constant, there is no appreciable change in the density of reaction mass). This set-up is used to study a catalytic homogeneous reaction under adiabatic condition.The set-up consists of a Dewar flask of capacity 1 lit. fitted with a stirrer. The flask is double insulated by ceramic wool insulation. Temp. is measured by digital temp indicator. The whole setup is mounted on a rigid M.S. frame.

EXPERIMENTATION:

Ø  To study the hydrolysis of acetic anhydride with water in presence of an acid catalyst (H₂SO₄).

Ø  To predict the degree of conversion from time-temperature data.

UTILITIES REQUIRED:

Ø  Instruments, Laboratory wares and Chemicals required for analysis as per the system adopted.

Ø  The whole unit is assembled rigidly on a base plate and mounted on a stand.

Ø  Most of the parts are powder coated and rest are painted with auto paints.

 TECHNICAL DETAILS :

Ø  Reactor : Material Stainless Steel, Capacity 1 Ltrs. (Approx) Insulated with Ceramic wool.

Ø  Stirrer : Teflon Impeller and Stainless Steel shaft coupled with FHP motor

Ø  Control panel comprises of : Digital Temp. Indicator : 0-199.9°C, RTD PT-100 type

Ø  Temp. Sensors : RTD PT-100 type With Standard make on/off switch, Mains Indicator etc.

Ø  Instruction Manual : An ENGLISH instruction manual will be provided along with the Apparatus

Ø  The whole unit is assembled rigidly on a base plate and mounted on a stand.

Ø  Most of the parts are powder coated and rest are painted with auto paints.

Additional Information:

• Item Code: SCRE-09
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: Wooden boxes are used.

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Present set-up consists of a reactor vessel fitted with variable speed agitator and detachable baffles. This unit is designed to study chemical kinetics. Reactants are fed to the reactor, using pump and flow is regulated and monitored by individual Rota meter. An adjustable overflow device is provided in the reactor to conduct the experiment on different reactor volume. A Stainless Steel Coil is immersed in the reactor through which the hot water supply is circulated. Temperature of the hot water is controlled by means of Temperature Controller and it enables the students to enhance the experimentation capabilities.

EXPERIMENTATION:

Ø To study the chemical kinetics.

Ø To study the effect of residence time.

Ø To study the effect of mixing speed.

Ø To study the effect of temperature on chemical reaction.

UTILITIES REQUIRED :

Ø Water Supply and drain.

Ø Table for set-up support.

Ø Instruments, Laboratory wares and Chemicals required for analysis as per the system adopted.

TECHNICAL DETAIL:

Ø Reactor Material : Acrylic/SS/Glas

Ø Capacity : Adjustable from 1 – 2 Ltrs

Ø Agitator : Variable speed with speed control facility 0-150 RPM

Ø Impeller: 4 Square bladed (1 No.)

Ø Material: Stainless Steel.

Ø Baffles: Detachable.

Ø Piping: PVC.

Ø Feed Tank (2 Nos.) Material : Acrylic/Stainless Steel/PVC

Additional Information:

• Item Code: SCRE-12
• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: wooden boxes are used.

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Additional Information:

• Production Capacity: 100 units/month
• Delivery Time: 10-15days
• Packaging Details: wooden boxes are used.